Hi mat, in that file there are 2 objects, the big one is a single surface and the fillet like one is a polysurface made up of 2 surfaces joined together.
The Rhino MergeSrf command only works on single surfaces, it won't allow you to select an object made up of multiple surfaces. You would need to use the Explode command on the multiple surface object to break it into individual surfaces before you'll be able to select it for merging.
But also you may need to cut that fillet surface in half because MergeSrf may not handle making a closed surface like that would form. You can use Split with the Isocurve and Shrink=yes options to cut the longer piece so it won't be trying to merge into a closed result.
- Michael
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